Influence of Substrate Temperature on Structural and Morphological Properties of SnO2 Nanostructured Thin Films

  • D. C. VLADU "Dunarea de Jos" University of Galati, Romania
  • C. GHEORGHIES "Dunarea de Jos" University of Galati, Romania
  • M. BERCEA U. T. Gh. Asachi Iasi, Romania
  • I. STOICA "Petru Poni" Institute of Macromolecular Chemistry Polymer Materials Physics, Romania
  • M. C. POPESCU National Institute for Research and Development in Microtechnologies IMT, Romania
  • B. BITA National Institute for Research and Development in Microtechnologies IMT, Romania
  • M. BORDEI "Dunarea de Jos" University of Galati, Romania
Keywords: electron beam-physical vapor deposition, structural, morphological properties, TEM, SEM, AFM

Abstract

SnO2 nanostructures thin films with thickness of 500 nm were prepared by electron beam-physical vapor deposition on glass substrate at temperature of 300, 373, 443, and 583 K. Structural and morphological properties of these nanostructured thin films were studied by Scanning and Transmission Electron Microscopy (SEM, TEM) and Atomic Force Microscope (AFM) methods. The changes in structural and morphological properties are found at different temperatures. Increase temperature causes important change of the structural and morphological properties. The sample prepared at 300 K has crystalline structure and the sample prepared at 583 K has amorphous structure. Roughness parameters have low values at 300, 373, 443 K as opposed to the values obtained at 583 K. This different behavior may be due to the amorphous structure of the sample that was observed in the TEM analysis.

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References

[1]. W. Gopel, K.D. Schierbaum - Sens. Actuators B 26 (1995) 1.
[2]. K.L. Chopra, S. Major, D.K. Pandya - Thin Solid Films 102 (1983) 1.
[3]. W.A. Badawy, H.H. Afify, E.M. Elgiar - J. Electrochem. Soc. 137 (1990) 1592.
[4]. A.K. Abbas, M.T. Mohammad - J. Appl. Phys. 59 (1986) 1641.
[5]. G. Sberveglieri - Sens. Actuators B: Chem. 6 (1992) 239.
[6]. A.F. Khan, M. Mehmood, A.M. Rana, M.T. Bhatti, A. Mahmood - Chin. Phys. Lett. 7 (2009) 077803.
[7]. A.F. Khan, M. Mehmood, A.M. Rana, M.T. Bhatti - Appl. Surf. Sci. 255 (2009) 8562.
[8]. I.H. Kim, J.H. Ko, D. Kim, K.S. Lee, T.S. Lee, J.-h. Jeong, B. Cheong, Y.-J. Baik, W.M. Kim - Thin Solid Films 515 (2006), 2475.
[9]. H.J. Kim, J.W. Bae, J.S. Kim, Y.C. Jang, G.Y. Yeom, N.E. Lee - Surf. Coat. Technol. 131 (2000) 201.
[10]. S.G.P. Boroojerdian, S.R. Sainkar, R.N. Karekar, R.C. Aiyer, S.K. Kulkarni - Thin Solid Films 295 1997) 271.
[11]. R. Cavicchi, S. Semancik - Thin Solid Films 206 (1991) 81.
[12]. I.A. Karapatnitski, K.A. Mit, D.M. Mukhamedshina, N.B. Beisenkhanov - Surf. Coat. Technol. 151–152 (2002) 76.
[13]. J.C. Jiang, K. Lian, E.I. Meletis - Thin Solid Films 411 (2002) 203.
[14]. S. Wang, J. Huang, Y. Zhao, S. Wang, S. Wu, S. Zhang, W. Huang - Mater. Lett. 60 (2006) 1706.
[15]. C.F. Wan, R.D. McGrath, W.F. Keenan, S.N. Frank - J. Electrochem. Soc. 136 (1989) 1459.
[16]. N. Tigau, V. Ciupina, G. Prodan, G.I. Rusu, E. Vasile - J.Cryst. Growth 269, 392, 2004.
[17]. M. Huang, Y. Wang, Y. Austin Chang - Thin Solid Films 449, 113, 2004.
[18]. D. E. Wolfe, M. Movchan and J. Singh - Architecture of Functionally Gradient Ceramic-Metallic Coatings By EBPVD for High Temperature Applications, Proceedings of Proceeding of Advances in Coating Technologies, at TMS Annual Meeting at Orlando, edited by C. R. Clayton and J. K. Hirvonen (TMS, 1997), p. 93.
[19]. D. E. Wolfe J. Singh and K. Narasimhan - J. Surf. Coat. Techn. 165 (2003) 8.
[20]. Y. Wang, S. Zhang, K. Wei, N. Zhao, J. Chen, X. Wang - Mater. Lett. 60 (2006) 1484.
[21]. H.N. Lim, R. Nurzulaikha, I. Harrison, S.S. Lim, W.T. Tan, M.C. Yeo - Int. J. Electrochem. Sci., 6 (2011) 4329-4340.
Published
2013-09-15
How to Cite
1.
VLADU DC, GHEORGHIES C, BERCEA M, STOICA I, POPESCU MC, BITA B, BORDEI M. Influence of Substrate Temperature on Structural and Morphological Properties of SnO2 Nanostructured Thin Films. The Annals of “Dunarea de Jos” University of Galati. Fascicle IX, Metallurgy and Materials Science [Internet]. 15Sep.2013 [cited 8Oct.2024];36(3):44-9. Available from: https://www.gup.ugal.ro/ugaljournals/index.php/mms/article/view/2743
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